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2 article(s) from Styring, Peter

Continuous-flow Heck synthesis of 4-methoxybiphenyl and methyl 4-methoxycinnamate in supercritical carbon dioxide expanded solvent solutions

Phei Li Lau,
Ray W. K. Allen and
Peter Styring

Beilstein J. Org. Chem. 2013, 9, 2886–2897, doi:10.3762/bjoc.9.325

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Scheme 1: General Heck reaction showing the possible isomers that can be produced.

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Figure 1: Schematic diagram of the stirred autoclave reactor. Pickel’s pump NWA PM101 was used to achieve sup...

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Figure 2: Schematic diagram of the continuous flow system. The reactor shown is the 3.9 mm i.d. PFR. For the ...

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Figure 3: Total conversion of 4-iodoanisole as a function of reactor run time for three reaction temperatures....

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Figure 4: Total conversion of 4-iodoanisole at 155 °C and 200 bar as a function of reactor run time for diffe...

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Figure 5: Total conversion of 4-iodoanisole as a function of reactor run time at 145 °C and at 200 (●) and 25...

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Figure 6: Conversion of 4-iodoanisole to methyl 4-methoxycinnamate (●) at 155 °C and 200 bar as a function of...

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Figure 7: Comparison of conversion as a function of reactor run time for the reaction of methyl acrylate in t...

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Figure 8: TOF values for the 1 mm (ο) and 3.9 mm (●) PFRs at a total flow rate of 0.12 mL min⁻¹, 155 °C and 2...

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Figure 9: Turnover frequencies of the Heck reactions at 155 °C using styrene (ο) as combined isomeric product...

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Full Research Paper

Published 17 Dec 2013

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From discovery to production: Scale- out of continuous flow meso reactors

Peter Styring and
Ana I. R. Parracho

Beilstein J. Org. Chem. 2009, 5, No. 29, doi:10.3762/bjoc.5.29

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Scheme 1: Synthesis of 4-methoxybiphenyl (4-MeOBP) and by-products in the Kumada reaction.

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Figure 1: Stainless steel single column flow reactor for discovery scale synthesis.

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Figure 2: (a): Schematic diagram of the parallel reactor housing (dimensions in mm); (b) the stainless steel ...

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Figure 3: Schematic diagram of the pneumatic pumping system.

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Scheme 2: Proposed catalytic cycles for the transformation of 4-haloanisole (Ar-X) and Grignard reagent (RMgX...

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Figure 4: Comparative study of flow rates in a single channel meso flow reactor. The output was sampled hourl...

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Figure 5: Kumada reaction carried out in a parallel channel meso reactor at a flow rate of 95 ml h⁻¹.

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Figure 6: Kumada reaction carried out in a parallel channel meso reactor over a 31-hour period at a flow rate...

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Figure 7: Kumada reaction carried out in a parallel channel meso reactor at a flow rate of 190 ml h⁻¹.

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Full Research Paper

Published 09 Jun 2009

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